Hitachi F7000 Instruction Manual
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1.4 Screen Composition 1 - 20 1.4.2 Kinds of Windows The FL Solutions 2.1 program has two kinds of windows: monitor window and data processing window. Fig. 1-33 Monitor Window 1 Monitor window Set the monitor window active for measurement. • The toolbar is now turned into the one for this window. Fig. 1-34 Data Processing Window 2 Data processing window Set the data processing window active for data processing. • The toolbar is now turned into the one for this window. 1 2
1.4.3 1 - 21 1.4.3 Data Processing Window The items displayable in each measurement mode are shown below. Fig. 1-35 Wavelength Scan 1 Wavelength scan • A spectrum alone can be displayed or both spectrum (①) and peak table (②) can be displayed as shown in Fig. 1-35. • Display of the peak table can be turned ON/OFF by the “Peak Table” command in the View menu. Fig. 1-36 Time Scan (kinetics result table) 2 Time scan • A spectrum alone can be displayed or both spectrum (③) and kinetics result table (④) can be displayed as shown in Fig. 1-36. Fig. 1-37 Time Scan (peak table) • Both spectrum (③) and peak table (⑤) can be displayed as shown in Fig. 1-37. • Display of the kinetics result table or peak table can be turned ON/OFF by the “Kinetics” or “Peak Table” command in the View menu. 1 2 3 4 5 3
1.4 Screen Composition 1 - 22 Fig. 1-38 3 Photometry • On start from measurement for a calibration curve, a window as shown in Fig. 1-38 will appear. Standard data (⑥) Calibration curve (⑦) Sample data (⑧) Calibration curve data (⑨) Fig. 1-39 • On sample measurement with a calibration curve generated through factor input, a window as shown in Fig. 1-39 will appear. Sample data (⑩) Calibration curve factor (⑪) Fig. 1-40 • On measurement of the photometric value at each wavelength in multi-wavelength mode, the sample data is displayed as listed in Fig. 1-40. Sample data (⑫) 9 76 8 10 11 12
1.4.4 1 - 23 1.4.4 Explanation of Tool Buttons The FL Solutions 2.1 program provides five kinds of toolbars as shown below. You can also select a command by pulling down each menu from the menu bar. But for quick and easy operation, it is advisable to use these tool buttons. Fig. 1-41 Toolbars Standard toolbar Has buttons related to printing and file handling. Instrument toolbar (displayed in monitor window) Has buttons related to spectrophotometer control such as wavelength drive and automatic pre- scanning. Measurement toolbar (displayed in monitor window) Has buttons related to measurement such as analysis method setting and sample name input. Spectrum toolbar (displayed in data processing window) Has buttons related to spectral display such as auto scaling, ruled line indication and spectrum tracing. Processing toolbar (displayed in data processing window) Has buttons related to data processing such as smoothing and differentiation. Fig. 1-42 An Example of Toolbar Arrangement 1 These five toolbars are independent and each of them can be located at a desired position as shown in Fig. 1-42 (monitor window). 1
1.4 Screen Composition 1 - 24 The following tables present the functional descriptions of the buttons on each toolbar. The function keys on the keyboard can also be utilized for the same purpose. For the functional assignment to each function key, refer to 1.5. Table 1-1 Standard Toolbar Button Function Button Function Creates a new analysis method/sample table. Opens the print window. Opens data files. Indicates the present status of the connected spectrophotometer. Opens a data file in the print preview mode. Indicates the information (version number, etc.) on the FL Solutions program. Saves the current file. Calls up the help window. Stores a selected character string or graphic item into the clipboard. Brings the monitor window to the forefront. Pastes the contents of the clipboard. Table 1-2 Measurement Toolbar Button Function Button Function Opens the Analysis Method window. Starts measurement. Displays the same name/comment entry window. Stops measurement. Displays the sample table. Closes the shutter. For manual input of standard sample values. Opens the shutter. Executes pre-scanning.
1.4.4 1 - 25 Table 1-3 Spectrum Toolbar Button Function Button Function Restores the scale to its original condition. For display in a contour map. Indicates ruled lines. For display from the front. Indicates a bird’s-eye view. For display from the left. For display from the rear. Automatically sets the scale. For display from the right side. Displays a dialog box to allow change of sample name/comment. Selects a spectrum to be displayed. Sets a mode for expansion of contour scale. For this expansion, click this icon and drag the area to be enlarged with the mouse. Indicates the trace cursor. Table 1-4 Instrument Toolbar Button Function Button Function Performs wavelength drive. Restores the scale to its original condition. Performs automatic pre-scanning. This is a function for automatic search of the optimum excitation and emission wavelengths for a sample. Adopts auto scale for vertical- axis display so that you can view the entire spectral graph. Conducts zero-point adjustment. Zero point with the shutter closed is adjustable. Effective for higher-accuracy measurement. Indicates ruled lines. Enlarges the vertical axis double. Magnifies the present data and status. Reduces the vertical axis to half.
1.4 Screen Composition 1 - 26 Table 1-5 Processing Toolbar Button Function Button Function Opens the Spectrum Properties window. Performs fundamental arithmetic calculations between spectra. Outputs a report of data file. Calculates the life of phosphorescence. Performs peak detection. Performs smoothing. Performs differentiation. Resets data. Performs peak detection in 3- dimensional measured data. Performs fundamental arithmetic calculations of 3-dimensional spectra. Performs area calculation.
1.5 1 - 27 1.5 Functions of Function Keys The function keys on the keyboard provides the following functions. Each function can be executed directly. Key No. Wavelength Scan Time Scan Photometry 3-D Scan 3-D Time Scan [F4] Measurement Measurement Sample measurement Measurement Measurement [F5] Blank measurement [F6] Stop Stop Stop Stop Stop [F7] Interrupting measurement [F8] Re- measurement [F9] End
1.6 Explanation of Monitor Window 1 - 28 1.6 Explanation of Monitor Window Fig. 1-43 1 Sample name indication A sample name is indicated. For its input, use the sample table or sample name/comment input window. 2 Current photometric value indication The current photometric value is indicated. 3 EX The current excitation wavelength is indicated. 4 EM The current emission wavelength is indicated. 5 EX slit The current excitation slit width is indicated. 6 EM slit The current emission slit width is indicated. 7 Shutter Open or closed state of the shutter is indicated. 8 Lamp ON/OFF state of the light source lamp is indicated. 9 Shutter control The active state of shutter control is indicated. 10 Corrected spectra Setting of spectrum correction is indicated. 11 Sample The number assigned to the sample under measurement is indicated. 12 Replicate count A count in repeated measurement is indicated. 2 1 3 4 7 8 9 10 11 12 13 14 5 6
1.6 1 - 29 13 Message indication A status message such as “Ready,” “Scanning” or “Parameter” is presented. In the “Ready” status, the (measurement) button can be clicked. 14 Error message indication An error message “Xe lamp” is presented. If any error message appears, take a proper countermeasure, referring to 4.7 of the maintenance edition.