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Hitachi F7000 Instruction Manual

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    							4.4.2 
    4 - 35 
    ②  To interrupt the measurement for other samples, put a check 
    mark for “Insert a new sample into the sequence?” as shown 
    in Fig. 4-38.    Then, click Yes.  
     
     
     
    Fig. 4-38 
     
     
    ③  The window in Fig. 4-39 appears.    Enter the sample name 
    and comment, and then click OK.  
     
     
     
    Fig. 4-39 
     
     
    2
    3 
    						
    							4.4  Conducting Measurement 
    4 - 36 
    ④  When you click OK, measurement of the interruption sample 
    starts.  
     
     
     
    Fig. 4-40 
     
     
    When measurement of all samples is over, the data 
    processing window shown in Fig. 4-41 will be displayed 
    automatically (only when “Open data processing window 
    after data acquisition” is selected at the Monitor tab in 
    Analysis Method).   
    After measurement of all the samples entered for Sample 
    Table, the photometric data will be saved automatically at the 
    specified saving location using the specified file name.   
     
     
    4 
    						
    							4.4.3 
    4 - 37 
    Upon completion of photometry or when opening the data file, the data 
    processing window is displayed as shown in Fig. 4-41.   
     
     
     
     
    Fig. 4-41    Data Processing Window (photometry) 
     
     
    ① Standard data  
    The measurement results of standards used for preparing a 
    calibration curve are displayed.   
     
     
     
    Fig. 4-41-1  Standard Data 
     
     
    ② Calibration curve  
    A calibration curve obtained from standard data is displayed.   
    The curve can also be traced.   
    Photometric value and Concentration are indicated at the top left 
    of this field.   
    4.4.3 Explanation of 
    Measurement 
    Result Window
    ①Standard data② Calibration 
    curve 
    ③Results of sample 
    measurement 
    ④ Calibration curve 
    data  
    						
    							4.4  Conducting Measurement 
    4 - 38 
    ③  Results of sample measurement 
    Sample data such as photometric value (Data), concentration 
    (Conc), mean value (Avg Conc), standard deviation (SD), 
    coefficient of variation (CV) and upper/lower limit judgment results 
    (HIGH/LOW) are displayed.   
     
     
     
    Fig. 4-41-2    Results of Sample Measurement   
     
     
    ④  Calibration curve data   
    Data such as determination coefficient and factors (A0, A1, A2, 
    A3) of calibration curve are displayed.    And the calibration type 
    can be changed.     
     
     
     
    Fig. 4-41-3    Calibration Curve Data 
     
      
    						
    							4.4.3 
    4 - 39 
    NOTICE:  1.  The data measured under the following conditions will 
    be saved automatically in Program Files\FL 
    Solutions\Data.  (Example:  C:Program Files\FL 
    Solutions\Data)  
    (1)  Measurement was carried out using a sample table 
    with no file name specified in the File Name 
    column.  
    (2)  Measurement was carried out with “Auto File” 
    specified and a file name unspecified, avoiding use 
    of a sample table.   
      2.  The data measured under the following conditions will 
    be saved automatically in Program Files\FL Solutions.   
    (Example:  C:Program Files\FL Solutions)  
    (3)  There is not an adequate free area in the specified 
    storage medium (such as floppy disk or MO).     
    (4)  Writing is inhibited.   
    A file automatically saved under such a condition as above is 
    named according to the following rule.   
    Rule 1:  When a file name is given to analysis method: 
    File name of analysis method + serial No. (001, 
    002, ...)   
    Rule 2:  When a file name is not given to analysis method:   
    DEFLT + serial No. (001, 002, ...)   
     
     
      
    						
    							4.4  Conducting Measurement 
    4 - 40 
    If remeasurement becomes necessary after completing a series of 
    measurements, both standard and sample data accept remeasurement.   
     
    ①  Click the data to be remeasured for making it active as shown in 
    Fig. 4-42.   
     
    NOTE:  Figure 4-42 shows the window for the case where the sample 
    table is not used.    Five buttons including the Remeasure(F8) 
    are displayed.    On the window for the case where the sample 
    table is used, only the Remeasure(F8) button is displayed.   
     
     
     
    Fig. 4-42  Measurement End Window   
    (without using sample table) 
     
     
    ② Click the Remeasure(F8) button.    A window as shown in Fig.   
    4-43 will appear.   
     
     
     
    Fig. 4-43 
     
    4.4.4 Re-
    measurement 
    3
    21 
    						
    							4.4.4 
    4 - 41 
    ③ Click OK, and measurement will start.    When standards are 
    remeasured, a calibration curve will be displayed through 
    recalculation of the data.   
     
    ④  For saving data after remeasurement, click the 
     button.  
    The data processing window appears.    From the File menu, 
    select “Save As” and save the data.   
     
    Remeasurement is possible for both standard and sample data.   
     
      
    						
    							4.4  Conducting Measurement 
    4 - 42 
    Statistical calculation ensues from sample measurement.    The results 
    are displayed in the “Avg Conc” column of the data processing window 
    as shown in Fig. 4-41-2.   
     
    MEANXN
    i=∑
     
    SDXXN
    Nii=
    ∑∑22
    1 () 
    CVSD
    MEAN =×100
     
     
    Here,  N  =  Number of standards   
     MEAN = Mean value  
     SD = Standard deviation  
      CV  =  Coefficient of variation (%)   
     
    NOTE: [∗∗∗∗∗] is indicated for SD and CV values when they are nearly 
    “0.”  
     
     
    4.4.5 Statistical 
    Calculation  
    						
    							4.5 
    4 - 43 
    4.5  Data Printout  
     
    Printout can be provided even when the function for automatic printout 
    after measurement is not used.    The following two procedures are 
    available.  
     
    (1)  Click on the spectrum window, and the circumference turns blue.   
    In this status, select the Print command from the File menu.     
    Or click the 
      (print) button on the toolbar.    The field active 
    on the data processing window (e.g., ②  in Fig. 4-41) will be 
    printed.    What is displayed by clicking the Print Preview 
    command in the File menu will be printed.   
     
     
     
    Fig. 4-44 
     
      
    						
    							4.5  Data Printout 
    4 - 44 
    (2)  Select the Report command in the Data menu.    Or click the  
    (report) button on the toolbar.    The Print Preview window will 
    appear as shown below.    For printout, click the Print button.   
    Measurement conditions will be printed together.   
     
     
     
    Fig. 4-45 
     
     
    Select the items to be printed at the Report tab with the 
    Photometry Properties command chosen in the Edit menu.   
     
     
     
    Fig. 4-46 
      
    						
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