Hitachi F7000 Instruction Manual

							2.5  Conducting Measurement 
2 - 24 
(5)  Upon completion of the measurement, the measured data will be 
saved automatically at the specified saving location using the 
specified file name.    Opening the saved data file will display the 
data processing window as shown below. 
 
 
 
Fig. 2-20    Data Processing Window (wavelength scan) 
 
 
① Spectrum  
The spectrum of a measured sample is displayed.   
 
② Peak table  
Peak wavelength, peak height and valley wavelength are 
listed.  
 
① Spectrum
②Peak table  
						

							2.5.2 
2 - 25 
NOTICE:  1.  The data measured under the following conditions will 
be saved automatically in Program Files\FL 
Solutions\Data.  (Example:  C:Program Files\FL 
Solutions\Data)  
(1)  Measurement was carried out using a sample table 
with no file name specified in the File Name 
column.  
(2)  Measurement was carried out with “Auto File” 
specified and a file name unspecified, avoiding use 
of a sample table.   
2.  The data measured under the following conditions will 
be saved automatically in Program Files\FL Solutions.   
(Example:  C:Program Files\FL Solutions)  
(3)  There is not an adequate free area in the specified 
storage medium (such as floppy disk or MO).     
(4)  Writing is inhibited.   
A file automatically saved under such a condition as above is 
named according to the following rule.   
Rule 1:  When a file name is given to analysis method: 
File name of analysis method + serial No. (001, 
002, ...)   
Rule 2:  When a file name is not given to analysis method:   
DEFLT + serial No. (001, 002, ...)   
 
  
						

							2.6  Data Printout 
2 - 26 
2.6  Data Printout  
 
Printout can be provided even when the function for automatic printout 
after measurement is not used.    The following two procedures are 
available.  
 
(1)  Click on the spectrum window, and the circumference turns blue.   
In this status, select the Print command from the File menu.     
Or click the 
  (print) button on the toolbar.    The field active 
on the data processing window (e.g., ①  in Fig. 2-20) will be 
printed.    What is displayed by clicking the Print Preview 
command in the File menu will be printed.   
 
 
 
Fig. 2-21   
 
 
(2)  Select the Report command in the Data menu.    Or click the 
 
button on the toolbar.    The Print Preview window will appear as 
shown below, so click Print.   
						

							2.6 
2 - 27 
 
 
 
Fig. 2-22 
 
 
NOTE:  If characters overflow from the print frame in repeat 
measurement or in overlaying, then change the printing 
orientation from vertical (Portrait) to horizontal (Landscape).   
  
						

							2.6  Data Printout 
2 - 28 
Select the items to be printed in the following procedure.   
Click the 
  button, and the Spectrum Properties window will appear.   
↓ 
Select the Report tab, and the window in Fig. 2-23 will open.   
↓ 
In this window, select desired print items.   
 
 
 
Fig. 2-23 
 
  
						

							3.1 
3 - 1 
3.  TIME SCAN  
 
3.1  Flow of Operation  
 
This section explains the parameter setting and operating method for 
time scan.    Measurement proceeds along the flow shown below.   
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
Fig. 3-1    Operational Flow (time scan) Click 
  button. 
 • Measuring wavelengths 
•  Scan time, etc. 
Click 
 button. 
 • Sample name 
• Auto File 
•  File name at destination of 
saving, etc. 
Set a sample.   
Click 
  button to execute time scan. 
• Rate calculation 
• Peak detection 
• Spectrum tracing 
• Spectral calculation 
Click 
  button.    Measurement result will be displayed 
in a report format. 
 
Start 
Method setting 
(See 3.2.) 
Sample name/ 
comment input 
(See 3.3.) 
Measurement 
(See 3.4.) 
Data processing 
(See Section 7.) 
Result output in report 
(See 3.5.) 
End  
						

							3.2    Creating an Analysis Method 
3 - 2 
3.2    Creating an Analysis Method   
 
Set the analytical conditions (method) prior to measurement.     
From the Edit menu, select the Method command or click the 
 
button.    A window shown in Fig. 3-2 will appear.   
 
 
 
Fig. 3-2  Analysis Method 
 
 
The following tabs are provided on the Analysis Method window for the 
time scan mode.    These tabs are detailed on the subsequent pages.   
• General  
• Instrument  
• Monitor  
• Processing  
• Report  
 
  
						

							3.2.1 
3 - 3 
The parameters shown in Fig. 3-3 are provided at the General tab.     
For the settable range of each parameter, refer to Appendix G.   
 
 
 
Fig. 3-3  General Tab 
 
 
1 Measurement (mode)   
A measurement mode is selectable.    Here, select “Time scan.”   
For Wavelength scan, Photometry, 3-D Scan and 3-D Time scan, 
refer to Sections 2, 4, 5 and 6, respectively.   
2 Operator  
Enter an operator name.   
3 Instrument  
The name of the connected instrument is indicated.   
4 Sampling  
- Standard   
Indicates that samples are to be exchanged manually.     
5 Comments  
Enter a description or notes on measuring conditions.   
6 Use sample table (Set measurement sample)   
Apply a check mark here when a sample table is used.   
3.2.1 General Tab 
 
1 
2 
3 
4 
5 
6 
7 
8 
9  
						

							3.2    Creating an Analysis Method 
3 - 4 
7 Load  
Click this button to read out saved analytical conditions.     
Upon clicking, the file opening window appears.    So, select an 
analytical condition file.   
8 Save  
When you click this button after setting the parameters, the 
analytical conditions can be saved by overwriting.    In case of a 
new analysis method, clicking this button displays the “Save As” 
window.    You must enter a file name for saving in this window.   
9 Save As   
Click this button for renaming the set conditions for saving.     
The “Save As” window appears, so enter a file name.   
  
						

							3.2.2 
3 - 5 
This window appears when Time scan is specified for Measurement at 
the General tab on the Analysis Method window.    When you click the 
Instrument tab, the window in Fig. 3-4 appears.   
For the settable range of each parameter, refer to Appendix G.   
 
 
 
Fig. 3-4  Instrument Tab  
 
 
1 Data mode   
Select a data mode.    The Luminescence mode is for measuring 
luminescence in the biological/chemical field.    In this mode, only 
the sample side signal is acquired without performing ratio 
photometry.    If phosphorescence life is shorter than 20 ms, 
“Phosphorescence short life” should be selected.    In this case, unit 
time and measuring time are automatically set to ms and 20 ms. 
2 Chopping speed   
Select a chopping speed.    Setting is allowed when 
Phosphorescence is selected for Data mode.     
The Phosphorescence mode is for acquiring only phosphorescence 
after extinction of excitation beam while turning a chopper on the 
excitation side.    An increase in chopping speed makes the 
chopper turns faster.   
3.2.2 Instrument Tab 
 
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