Hitachi F7000 Instruction Manual

							8.13    Display of Monitor Window at Forefront 
8 - 26 
8.13    Display of Monitor Window at Forefront 
 
In repeat measurement or use of the autosampler, the monitor window 
may not be located because some spectral data processing windows 
are overlaid as shown in Fig. 8-33. 
 
 
 
Fig. 8-33 
 
 
Click the 
  button on the Standard toolbar.    The monitor window 
will be displayed at the forefront. 
 
 
 
Fig. 8-34 
  
						

							9.1.1 
9 - 1 
9.  MEASUREMENT USING OPTIONAL 
ACCESSORIES 
 
For how to connect the cable for each accessory, refer to the instruction 
manual attached to the accessory. 
Given below is the description of operations after setting of your analysis 
method, which is required as instructed in Sections 2 to 6. 
 
 
9.1    Use of Sample Sipper 
 
Hook up the sample sipper to the spectrophotometer. 
The parameters for the sample sipper are settable on its front panel. 
Explained here is the procedure for creating a calibration curve and 
measuring an unknown sample in the photometry mode. 
 
 
A message box appears in the standard measurement session, so 
operate in accordance with the messages.    A message box does not 
appear in the sample measurement session.    Measurement can be 
started just by pressing the sipping lever of the sample sipper. 
 
NOTES:  1.  In use of the sample sipper, remeasurement, interrupt 
measurement and blank measurement cannot be made.   
But remeasurement of standards is possible. 
  2.  When repeat measurement is set, the standards are 
measured by the set number of times.    Samples are 
measured only once. 
 
9.1.1 When Not 
Using Sample 
Table 
  
						

							9.1    Use of Sample Sipper 
9 - 2 
Select the Measure command from the Spectrophotometer menu or 
click the 
  (measurement) button on the toolbar.    A window as in 
Fig. 9-1 will open. 
 
 
 
Fig. 9-1 
 
 
Press the sipping lever.    Measurement will start.    Upon completion of 
the 1st standard measurement, a message box for the 2nd standard 
measurement will appear. 
For remeasurement or skipping, select the relevant item with the mouse 
(by placing a bullet in its radio button) and click Yes.  When you click 
No, the current measurement sequence is terminated. 
For restarting measurement, click the 
 button.  Measurement then 
starts from standard 1. 
Upon completion of standard measurement, a window as in Fig. 9-2 will 
appear.  
						

							9.1.1 
9 - 3 
 
 
 
Fig. 9-2 
 
 
By clicking OK, a calibration curve is drawn and then samples can be 
measured.    When a window as in Fig. 9-3 appears, press the sipping 
lever.    The result of measurement will appear in the area indicated by 
①  in Fig. 9-4. 
 
 
 
Fig. 9-3 
  
						

							9.1    Use of Sample Sipper 
9 - 4 
 
 
 
Fig. 9-4 
 
 
Upon completion of measurement, click the End button.    The data will 
be saved. 
 
For remeasuring any of the standards after their measurements, click its 
data as shown in Fig. 9-5.    Then click the Remeasure button. 
 
 
 
Fig. 9-5 
 
 
①  
						

							9.1.2 
9 - 5 
A message box as in Fig. 9-6 will open.    Press the sipping lever. 
 
 
 
Fig. 9-6 
 
 
When a standard is remeasured, the calibration curve is recalculated 
and sample data is also recalculated based on the curve and then 
displayed.    To save the recalculated data, click the End button or the 
  (save) button on the toolbar. 
 
 
A message box is displayed in both standard and sample measurement 
sessions.    So operate according to the messages.    When the 
message box appears, press the sipping lever of the sample sipper. 
 
NOTE:  When the sample sipper is used, blank measurement cannot 
be made. 
 
Select the Measure command from the Spectrophotometer menu or 
click the 
  (measurement) button on the toolbar.    A window as in 
Fig. 9-7 will open. 
 
 
 
Fig. 9-7 
9.1.2 When Using 
Sample Table 
  
						

							9.1    Use of Sample Sipper 
9 - 6 
Press the sipping lever.    Measurement will start.    Upon completion of 
the 1st standard measurement, a message box for the 2nd standard 
measurement will appear.    For remeasurement or skipping, select the 
relevant item with the mouse (by placing a bullet in its radio button), and 
then click Yes.  When you click No, the current measurement 
sequence is terminated. 
For restarting measurement, click the 
 button.  Measurement then 
starts from standard 1.   
 
Upon completion of standard measurement, a window as in Fig. 9-8 will 
open. 
 
 
 
Fig. 9-8 
 
 
By clicking OK with the mouse, a calibration curve is drawn and then 
samples can be measured. 
 
In case of sample measurement also, a message box as in Fig. 9-9 will 
appear.    Press the sipping lever.    Measurement of sample 1 will start.  
						

							9.1.2 
9 - 7 
 
 
 
Fig. 9-9 
 
 
For measurement of sample 2, a message box as in Fig. 9-10 will open. 
 
 
 
Fig. 9-10 
 
 
For measurement of sample 2, press the sipping lever. 
For skipping this sample (measurement of sample 3), select “Skip this 
sample?” and click the Yes button with the mouse. 
For remeasurement, select “Repeat the last measurement?” and click 
the Yes button with the mouse.    When repeat measurement has been 
set, measurement starts from the 1st one (Repl. No. 1) for the sample. 
  
						

							9.1    Use of Sample Sipper 
9 - 8 
In case of interrupt measurement, select “Insert a new sample into the 
sequence?” and click the Yes button with the mouse.    A message box 
as in Fig. 9-11 will appear.    Input a sample name and comment, and 
then click the OK button. 
 
 
 
Fig. 9-11 
 
 
For remeasurement after a series of measurements, click the data to be 
remeasured as shown in Fig. 9-12.    Then lick the Remeasure button. 
 
 
 
Fig. 9-12 
 
  
						

							9.1.3 
9 - 9 
A window as in Fig. 9-13 will open.    Press the sipping lever, and 
measurement will start.    When a standard is remeasured, the 
calibration curve is recalculated and sample data is also recalculated 
based on the curve and then displayed.    To save the recalculated data, 
click the 
 (save) button. 
 
 
 
Fig. 9-13 
 
 
(1)  When Not Using Sample Table 
 
Set your analysis method.    When the monitor window appears, 
press the sipping lever.    Measurement will start. 
 
(2)  When Using Sample Table 
 
Select the Measure command from the Spectrophotometer menu 
or click the 
  (measurement) button on the toolbar.     
A message box will appear.    Follow the messages given. 
 
 
9.1.3 In Wavelength 
Scan or Time 
Scan Mode