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Hitachi F7000 Instruction Manual

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    							7.12.1 
    7 - 27 
    7.12  Area Calculation 
     
    An area value is obtainable by integration in the specified range of the 
    presently displayed spectrum. 
    Click the 
      (area calculation) button on the Processing toolbar.     
    A window as in Fig. 7-32 will appear. 
    (Or select the Area command from the Data menu.) 
     
     
     
    Fig. 7-32 
     
     
    The range for area calculation is settable in the following two ways. 
     
    (1)  Setting by Moving Cursor 
     
    ① Click the Start button.  (Refer to ① in Fig. 7-33.)   
    Move the trace cursor to a desired start wavelength on the 
    spectrum (refer to ②  in Fig. 7-33), and then click the right 
    button of the mouse. 
     
    ② Click the End button.  (Refer to ③ in Fig. 7-33.)  Move the 
    trace cursor to a desired end wavelength on the spectrum 
    (refer to ④  in Fig. 7-33), and then click the right mouse 
    button. 
     
    7.12.1 Setting of 
    Calculation 
    Range 
      
    						
    							7.12  Area Calculation 
    7 - 28 
    ③ Click the Calculate button.    The result of calculation will be 
    indicated.  (Refer to ⑤  in Fig. 7-33.) 
     
     
     
    Fig. 7-33 
     
     
    (2)  Setting by Entering Numerical Value 
     
    ① Enter a desired start wavelength in the Start input box from 
    the keyboard. 
     
    ② Enter a desired end wavelength in the End input box from 
    the keyboard. 
     
    ③ Click the Calculate button.    The result of calculation will be 
    indicated. 
     
    1
    3
    5
    2
    4Calculation 
    result  
    						
    							7.12.1 
    7 - 29 
    (3)  The principle of area calculation is shown below. 
     
     
     
     
    Fig. 7-34    Principle of Calculation 
     
     
    The elements (D
    1 to Dn) of a spectrum are subjected to the 
    following calculation for obtaining an area value. 
     
    S
    3 = S1 + S2 = Sa + Sc + Sd 
    = {D
    2 + D3 +  Dn-2 + Dn-1 + (D1 + Dn)/2∗∆λ 
    S
    2 = Sb + Sd 
    = [(D
    1 + Dn)∗{∆λ∗ (n – 1)}]/2 
    = [(D
    1 + Dn)∗{section start wavelength (WL1) –   
    section end wavelength (WL
    2)}]/2 
    S
    1 = S3 – S2 
    D
    1:    Spectral data at section start wavelength 
    D
    n:    Spectral data at section end wavelength 
    ∆λ:  Sampling interval 
     
    In the time scan mode, change as follows. 
    Start wavelength (WL
    1) → End time (T2) 
    End wavelength (WL
    2) → Start time (T1) 
     
     
     D
    n-1
    Dn
    D2
    D1
    ∆λ
    S
    1
    S2
    WL1WL2WL1WL2  S
    a
    Sb Sc 
    S
    d
    Section end wavelength Specified rangeSection start wavelength  
    						
    							7.12  Area Calculation 
    7 - 30 
    The result of area calculation can be printed out. 
     
    (1)  To print a spectrum and the result of area calculation, put a check 
    mark at “Print spectrum.”    (Refer to ① in Fig. 7-35.)  To avoid 
    printing a spectrum, remove the check mark. 
     
    (2) Click Print to start printing.    (Refer to ② in Fig. 7-35.)   
    Upon execution of printing, the Area window will close.     
    The same window can be called up by clicking the 
     (area 
    calculation) button on the Processing toolbar. 
     
     
     
    Fig. 7-35 
     
     
     
     
     
    Fig. 7-36    Example of Printout (with spectrum record) 
     
    7.12.2 Printing of 
    Calculation 
    Result 
     
    1
    2
    3  
    						
    							7.12.2 
    7 - 31 
    (3)  Upon clicking the OK button after calculation (refer to ③ in Fig. 
    7-35), its result is saved although the Area window is closed. 
     
    (4)  The result of calculation is reset by clicking the 
     (reset) 
    button on the Processing toolbar with the data processing window 
    displayed.    Upon calling up the Area window again, therefore, 
    “*****” will be indicated in each result box. 
     
    NOTE:  Upon execution of file saving after area calculation, its result is 
    also saved in a file.    So a numerical value is indicated in each 
    result box when the Area window is called up.    These values 
    cannot be erased by clicking the reset button because they are 
    saved in the computer. 
     
      
    						
    							7.12  Area Calculation 
    7 - 32 
    For expanding the scale in the Area window, use the left button of the 
    mouse. 
     
    (1)  As shown in Fig. 7-37, specify an area to be expanded by drawing 
    a rectangle with the mouse while holding down its left button on a 
    spectrum. 
     
     
     
    Fig. 7-37 
     
     
    (2)  Then release the left button.    The specified area will be 
    expanded as shown in Fig. 7-38. 
     
     
     
    Fig. 7-38 
     
     
    (3)  Double clicking the left mouse button on the spectrum returns the 
    scale to the original one. 
    7.12.3 Scale 
    Expansion 
      
    						
    							7.13 
    7 - 33 
    7.13    Transfer of Data to Microsoft(R) Excel 
     
    Measured data can be transferred to a worksheet of Microsoft(R) Excel 
    in the following procedure. 
     
    (1) Click the 
      (properties) button and select the Report tab.     
    A tab page as in Fig. 7-39 will open.    Select “Use Microsoft(R) 
    Excel” for Output.    Also select data to be transferred (peak table, 
    data listing, etc. in case of wavelength scan).    Then click OK. 
     
     
     
    Fig. 7-39 
     
     
    (2) Click the 
      (report) button.    The Microsoft(R) Excel will 
    automatically start to read data.    The subsequent procedure 
    concerns the Microsoft(R) Excel operation. 
     
     
     
    Fig. 7-40  
    						
    							7.13    Transfer of Data to Microsoft(R) Excel 
    7 - 34 
    (3)  Data can be saved with extension code “xls” of Microsoft(R) Excel.   
    Select File – Save Copy As and enter a file name. 
     
     
     
    Fig. 7-41 
     
     
    (4)  Upon closing the Microsoft(R) Excel, a window as in Fig. 7-42 
    appears.    Now close this window.    The original data processing 
    window will appear again. 
     
     
     
    Fig. 7-42 
     
      
    						
    							7.14 
    7 - 35 
    7.14    Pasting of Spectrum to Microsoft(R) Word 
     
    A spectrum can be pasted to a Microsoft(R) Word text as it is.     
    Take the following procedure. 
     
    (1)  Make spectral data active by clicking the relevant spectrum in the 
    data processing window.    The thick frame will change to blue. 
     
    (2)  Select the Copy command from the Edit menu. 
     
    (3)  Open a Microsoft(R) Word text and click a position for pasting.     
    By clicking the Paste command from the Edit menu, the spectrum 
    can be pasted to the Microsoft(R) Word text. 
     
    Peak tables and/or kinetics data can also be pasted to a Microsoft(R) 
    Word text in the same way.    In this case, they are pasted as a text. 
    By double-clicking the pasted spectrum, functions such as scale change 
    and gridline indication are applicable. 
     
     
     
    Fig. 7-43    Spectrum Pasted to Microsoft(R) Word 
     
     
    Upon right-clicking the pasted spectrum, a menu box as in Fig. 7-48 will 
    appear to enable scale change, etc.    Any change made here is brought 
    into a Microsoft(R) Word text. 
     
    NOTE:  Editing in the Microsoft(R) Word can be made with a PC in 
    which the Microsoft(R) Word and FL Solutions program are 
    installed. 
     
      
    						
    							7.15    Pasting of Spectrum to Microsoft(R) Excel 
    7 - 36 
    7.15    Pasting of Spectrum to Microsoft(R) Excel 
     
    A spectrum can be pasted to the Microsoft(R) Excel as it is.   
    Take the following procedure. 
     
    (1)  Make spectral data active by clicking the relevant spectrum on the 
    data processing window.    The thick frame will change to blue. 
     
    (2)  Select the Copy command from the Edit menu. 
     
    (3)  Open the Microsoft(R) Excel and select “Paste Special” from its 
    Edit menu.    A dialog box as in Fig. 7-44 will open.    Make sure 
    that “FL Wavelength Scan Object” is indicated in “As.” 
     
     
     
    Fig. 7-44 
     
     
    (4) Click OK.    The spectrum will be pasted to the Microsoft(R) Excel. 
     
    Peak tables and kinetics data can also be pasted to the Microsoft(R) 
    Excel in the same way.    In this case, they are pasted as data for each 
    cell. 
     
      
    						
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