Hitachi F7000 Instruction Manual
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4.3.2 4 - 25 Fig. 4-21 4 Make entries for Sample and Comments of each sample. Maximum number of characters to be entered (half-size) Sample : 40 characters Comment : 255 characters Next, you must enter a file name for automatic saving after measurement. Click the […] button, and specify a saving location and enter a file name. Fig. 4-22 3 4 5 67 8
4.3 Defining Your Samples 4 - 26 5 After entries, check them and then click the OK button. 6 Load button Used for reading out the existing sample table. Clicking the Load button displays the file opening dialog. Fig. 4-23 File Opening Dialog Select a sample table and click the Open button. The specified sample table will be read out. 7 Save button The contents of change can be saved by overwriting. In case of a new generation, the Save As dialog will open. 8 Save As button Used for saving the sample table with a name newly given. Click this button, and the Save As dialog will open.
4.3.2 4 - 27 Fig. 4-24 Save As Dialog Select a saving location and enter a file name. Then, click the Save button.
4.4 Conducting Measurement 4 - 28 4.4 Conducting Measurement First create a calibration curve, and then proceed to sample measurement. (1) Click , select the Standards tab and make sure standards have already been defined. (Refer to 4.2.4.) Click the button or button to also confirm that the samples have already been defined. (Refer to 4.3.) (2) Click the (measurement) button to start measurement. When measurement starts, the window in Fig. 4-25 appears. Fig. 4-25 (3) When you click Yes, and the window in Fig. 4-26 will appear. Fig. 4-26 4.4.1 Standards Measurement
4.4.1 4 - 29 Set standard sample 1 and click OK. This standard sample is measured and advance to the next standard measurement is awaited. Since a window as shown in Fig. 4-25 appears, you should click Yes. Then, a window as shown in Fig. 4-26 appears. Set the next standard sample and click OK. Continue standard measurement until the standards set at the Standards tab in Analysis Method are all measured. (4) When measurement of all standards is finished, a window as shown in Fig. 4-27 appears. Clicking of the OK button under selection of “Go to measure samples” takes you to measurement of unknown samples. Fig. 4-27
4.4 Conducting Measurement 4 - 30 Now let’s measure samples. Operation differs between when a sample table is used and when it is not used. (1) Without using a sample table (when “Use sample table” is not selected in Analysis Method) Fig. 4-28 ① Set a sample and click the Sample(F4) button. Measurement is carried out and the result is displayed. ② For blank measurement at the mid-point of sample measurement, click Blank(F5). ③ To interrupt the measurement for other samples, click the Interrupt(F7) button. The window in Fig. 4-29 will appear. Enter a number for Interrupt’s Sample No. Fig. 4-29 4.4.2 Sample Measurement 1 236 4
4.4.2 4 - 31 ④ Click the OK button, and the window in Fig. 4-30 will appear. Fig. 4-30 ⑤ Click the OK button, and measurement of the interruption sample starts. ⑥ When sample measurement is finished, click the End(F9) button. When auto saving is selected, the measured data will be saved automatically at the specified saving location using the specified file name. When auto saving is not selected, you must select the “Save As” command from the File menu to save the measured data. Entry and Change of Sample Name After completion of sample measurement, sample names can be entered on the monitor window (Fig. 4-31). Fig. 4-31 Follow steps (a) to (d). 5
4.4 Conducting Measurement 4 - 32 (a) Select Edit Sample Name from the Edit menu as shown in Fig. 4-32. Fig. 4-32 (b) The Edit Sample Name dialog opens as shown in Fig. 4-33. Fig. 4-33
4.4.2 4 - 33 (c) Enter sample names as exemplified in Fig. 4-34 and click the Update or OK button. Fig. 4-34 (d) The monitor window is redisplayed with the newly entered sample names as shown in Fig. 4-35. Fig. 4-35 For saving the data after entry of sample names, click the button. The data processing window appears. Select the Save As command from the File menu and save the data. For changing the sample names, follow the same procedure as for entry of sample names.
4.4 Conducting Measurement 4 - 34 (2) With sample table (when “Use sample table” is selected in Analysis Method) Fig. 4-36 ① The message box shown in Fig. 4-37 appears. Carry out operation according to the messages. Measurement can be continued by clicking Yes and OK alternately. Fig. 4-37 1