Hitachi F7000 Instruction Manual
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3.5 Data Printout 3 - 26 3.5 Data Printout Printout can be provided even when the function for automatic printout after measurement is not used. The following two procedures are available. (1) Click on the spectrum window, and the circumference turns blue. In this status, select the Print command from the File menu. Or click the (print) button on the toolbar. The field active on the data processing window (e.g., ① in Fig. 3-20) will be printed. What is displayed by clicking the Print Preview command in the File menu will be printed. Fig. 3-23 (2) Select the Report command in the Data menu. Or click the (report) button on the toolbar. The Print Preview window will appear as shown below, so click Print.
3.5 3 - 27 Fig. 3-24 NOTE: If characters overflow from the print frame in repeat measurement or in overlaying, then change the printing orientation at the Report tab shown in Fig. 3-25 from vertical (Portrait) to horizontal (Landscape).
3.5 Data Printout 3 - 28 Select the items to be printed in the following procedure. Click the button, and the Spectrum Properties window will appear. ↓ Select the Report tab, and the window in Fig. 3-25 will open. ↓ In this window, select desired print items. Fig. 3-25
3.6 3 - 29 3.6 Calculating the Phosphorescence Life This is the function for calculating phosphorescence life from the measurement result (phosphorescence attenuation curve). Replacing data value at T1 with I 0, I0/e time (T2) is found, and T1, T2 and τ (phosphorescence life) = T2 - T1 are displayed. Select the phosphorescence life command from the Data menu or click the button on the Processing toolbar. A window as shown in Fig. 3-26 will appear. Fig. 3-26 Move the line cursor to the start point (T1) of calculation by the mouse or arrow keys [←] and [→] on the keyboard. Right-click the mouse at the start point. Or enter a numeral in the T1 field and click Calculate. The result of calculation will be displayed.
3.6 Calculating the Phosphorescence Life 3 - 30 Fig. 3-27 For printout of the calculation result, click Print. For printout of the spectrum and calculation result, apply a check mark to “Print spectrum” and click Print. For scale expansion, specify the area to be enlarged with the mouse. Draw a rectangle with the mouse button held down as shown in Fig. 3-28. Fig. 3-28
3.6 3 - 31 When releasing the mouse button, the specified area will be enlarged as shown in Fig. 3-29. Fig. 3-29 Double-clicking on the spectrum selects auto scale.
4.1 4 - 1 4. PHOTOMETRY 4.1 Flow of Operation This section explains the method of determining sample concentration with a calibration curve prepared. Measurement proceeds along the flow shown below. Fig. 4-1 Operational Flow (photometry) Click button and set an analysis method. • Quantitation type • Number of wavelengths • Calibration type Click button and set sample information. • Sample name • Auto File • File name at destination of saving, etc. Click and measure a standard sample according to the message guide. After completion of standard measurement, set a sample and click [Sample (F4)] button to measure the sample. Click button. Measurement result will be displayed in a report format. Start Method setting (See 4.2.) Sample name/ comment input (See 4.3.) Standards measurement (See 4.4) Sample measurement (See 4.4.) Result output in report (See 4.5.) End Standard table setting (See 4.2.) At the Standards tab, set a standard table.
4.2 Creating an Analysis Method 4 - 2 4.2 Creating an Analysis Method Set the analytical conditions (method) prior to measurement. From the Edit menu, select the Method command or click the button. A window shown in Fig. 4-2 will appear. Fig. 4-2 Analysis Method The following tabs are provided on the Analysis Method window for the photometry mode. These tabs are detailed on the subsequent pages. • General • Quantitation • Instrument • Standards • Monitor • Report
4.2.1 4 - 3 The parameters shown in Fig. 4-3 are provided at the General tab. For the settable range of each parameter, refer to Appendix G. Fig. 4-3 General Tab 1 Measurement (mode) A measurement mode is selectable. Here, select “Photometry.” For Wavelength scan, Time scan, 3-D Scan and 3-D Time scan, refer to Sections 2, 3, 5 and 6, respectively. 2 Operator Enter an operator name. 3 Instrument The name of the connected instrument is indicated. 4 Sampling - Standard Indicates that samples are to be exchanged manually. 5 Comments Enter a description or notes on measuring conditions. 6 Use sample table (Set measurement sample) Apply a check mark here when a sample table is used. 4.2.1 General Tab 1 2 3 4 5 6 7 8 9
4.2 Creating an Analysis Method 4 - 4 7 Load Click this button to read out saved analytical conditions. Upon clicking, the file opening window appears. So, select an analytical condition file. 8 Save When you click this button after setting the parameters, the analytical conditions can be saved by overwriting. In case of a new analysis method, clicking this button displays the “Save As” window. You must enter a file name for saving in this window. 9 Save As Click this button for renaming the set conditions for saving. The “Save As” window appears, so enter a file name.