Hitachi F7000 Instruction Manual
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6.2.5 6 - 11 Select the Report tab, and the window in Fig. 6-7 will appear. For the settable range of each parameter, refer to Appendix G. Fig. 6-7 Report Tab 1 Output • Print Report A report will be printed. For printing method, refer to 6.9. • Use Microsoft(R) Excel Data will be transferred to Microsoft (R) Excel. For transferring method, refer to 7.13. • Use print generator sheet Select this method for using the report generator (option). For usage, refer to the instruction manual of the report generator. 2 Orientation Selectable when Print Report is chosen for Output. Select a printing orientation. Either Portrait or Landscape orientation is selectable. When the Landscape orientation is selected, date and method can be printed. 6.2.5 Report Tab 4 3 1 2
6.2 Creating an Analysis Method 6 - 12 3 Print items (printable/transferable items) • Include date • Include instrument • Include graph When you put a check mark for this item, any of the graphs listed below is selectable. ◊ Contour ◊ Bird’s-eye view ◊ Contour and Bird’s-eye view ◊ Contour and Spectrum • Data listing ◊ Interval ◊ Start ◊ End These parameters are settable when “Use Microsoft(R) Excel” or “Use print generator sheet” is specified for Output. For time scan, make entries for Interval, Start and End. For wavelength scan, make entries for Interval, Start and End. 4 Printer Font Click the Select button for changing the font to be used in the report.
6.3 6 - 13 6.3 Defining Your Samples A sample must be defined in the following procedure before measurement. (1) Click the (sample name/comment input) button on the Measurement toolbar. The window in Fig. 6-8 will appear. Fig. 6-8 (2) Make entries for Sample name and Comment. Maximum number of enterable characters (half-size) Sample name : 40 characters Comment : 255 characters For automatic saving, put a check mark in the “Auto File” box to specify a file name. First click the Select button, and then specify a saving location and enter a file name. When you put a check mark at each head of “Auto Text file” and “Auto Meta file” after turning on “Auto File,” 3-D time scan data can be saved automatically in the following file formats as soon as this data is automatically saved. • ASCII text file (*.txt) • Graph meta file (*.wmf) The data will be saved in the file name entered for “File name.” (3) After completion of setting, click OK.
6.4 Conducting Measurement 6 - 14 6.4 Conducting Measurement (1) Make sure an analysis method has been set and a sample has been defined. (Refer to “6.2 Creating an Analysis Method” and “6.3 Defining Your Samples.”) (2) Set a sample in the sample compartment and click the button on the Measurement toolbar to start measurement. (See ① in Fig. 6-9.) On this monitor window, the X and Y axes stand for the EM-side wavelength and time (s), respectively. Fig. 6-9 Monitor Window (3) For halting the measurement midway, click the (stop) button on the toolbar. (See ② in Fig. 6-9.) (4) When measurement is completed, the data processing window appears as shown in Fig. 6-10. This is available only when a check mark is put for “Open data processing window after data acquisition” at the ‘Monitor’ tab of Analysis Method. (See ④ in Fig. 6-5.) The measured data will be saved automatically when auto saving is selected. 1 2
6.4 6 - 15 If auto saving is not selected, select the “Save As” command from the File menu and save the data. Opening the saved data file will display the data processing window as shown below. Fig. 6-10 Data Processing Window (3-D time scan) ① Contour lines From these contour lines, the time-scan spectrum and emission, excitation or synchronous spectrum can be read out. As the cursor is moved, the cursor-specified time scan spectrum and emission, excitation or synchronous spectrum are displayed in ② and ③. ② Time scan spectrum A time scan spectrum at the cursor position in ① is displayed. Wavelength and photometric value can be read by selecting the “trace” command from the View menu or clicking the button. ③ Emission spectrum (excitation spectrum, synchronous spectrum) An emission spectrum (excitation spectrum, synchronous spectrum) at the cursor position in ① is displayed. Wavelength and photometric value can be read by selecting the “trace” command from the View menu or clicking the button. ① Contour lines ②Time scan spectrum ③Emission spectrum ④ Peak table
6.4 Conducting Measurement 6 - 16 ④ Peak table Peak wavelength and peak height are indicated. For setting threshold and sensitivity values, click the button. NOTICE: 1. The data measured under the following condition will be saved automatically in Program Files\FL Solutions\Data. (Example: C:Program Files\FL Solutions\Data) (1) Measurement was carried out with “Auto File” specified and a file name unspecified. 2. The data measured under the following conditions will be saved automatically in Program Files\FL Solutions. (Example: C:Program Files\FL Solutions) (2) There is not an adequate free area in the specified storage medium (such as floppy disk or MO). (3) Writing is inhibited. A file automatically saved under such a condition as above is named according to the following rule. Rule 1: When a file name is given to analysis method: File name of analysis method + serial No. (001, 002, ...) Rule 2: When a file name is not given to analysis method: DEFLT + serial No. (001, 002, ...)
6.5 6 - 17 6.5 Displaying Data in a Bird’s-Eye View “3-D Time scan” data can be displayed in a bird’s-eye view. Select the (bird’s-eye view) button on the Spectrum toolbar. (Or select the bird’s-eye view command from the View menu.) Fig. 6-11 Viewing direction is changeable by clicking (from front), (from rear), (from left) or (from right). Clicking (contour line diagram) displays a contour line diagram.
6.6 Contour Scale Expansion with Mouse 6 - 18 6.6 Contour Scale Expansion with Mouse In the contour display of 3-D time scan data, display scale can be expanded with the mouse. On the Spectrum toolbar, click the (contour scale expansion) button. The button is set in the clicked status. Fig. 6-12 Move the mouse cursor onto the contour as shown in Fig. 6-13 and drag the mouse along an area to be expanded with the left mouse button held down.
6.6 6 - 19 Fig. 6-13 The area enclosed with the mouse cursor is now expanded as shown in Fig. 6-14. For restoring the original display, click the (scale reset) button. Fig. 6-14 For using the trace cursor on the contour window, click again for returning to the non-clicked status.
6.7 Auto Scale Display of Data 6 - 20 6.7 Auto Scale Display of Data When you click the (auto scale) button on the data processing window after completion of measurement or from which the 3-D time scan data file has been read out, the contour window, excitation spectrum window and emission spectrum window are displayed in the auto scale mode as shown in Fig. 6-16. Fig. 6-15 (Before execution of auto scale) Fig. 6-16 (After execution of auto scale) For restoring the original display, click the (scale reset) button.