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Hitachi F 2500 Manual

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    							7 - 11 
    7.7    Saving of Sample Table   
     
    Sample tables can be saved.     
    This is convenient for editing the sample table under the same 
    name each time.   
     
     
     
    Fig. 7-16  Sample Table 
     
     
    After editing the sample table, click Save As and the window in 
    Fig. 7-16 will appear.    Enter a file name.    For calling out the 
    saved file (*.fls), click Load and select the file.   
     
     
     
    Fig. 7-17 
    7.7  
    						
    							7 - 12 
    7.8    Change of Window Display   
     
    When selecting the View (V) menu, display/non-display of 
    toolbars and method of displaying multiple spectra can be 
    selected.  
     
     
     
     
     
     
     
     
     
     
     
     
     
     
     
    Monitor window  Data processing window 
     
    Fig. 7-20    View Menu Commands 
     
     
    Scale Y Axis Up  :  Y axis scale is doubled for 
    display.  
     
    Scale Y Axis Down  :  Y axis scale is contracted by half 
    for display.   
     
    Reset Y Axis, Reset Axes  :  The scale set under the Monitor 
    tab is taken.     
     
    Autoscale Y Axis, Autoscale :  Scale is adjusted to spectrum 
    size for display.     
    Display/ 
    non-display 
    setting  7.8    Change of Window Display  
    						
    							7 - 13 
    The method of displaying multiple spectra is selectable.   
     
     Overlay 
     
     
     
    Fig. 7-21 
     
     
     Stack 
     
     
     
    Fig. 7-22 
     
     
    7.8  
    						
    							7 - 14 
     Tile 
     
     
     
    Fig. 7-23 
     
    NOTE:  When six, seven or more spectra are displayed, there 
    is a possibility of the spectra becoming too small, or not 
    all the traced values can be displayed.    In this case, 
    use the Overlay (O) command of Data (D) menu to 
    delete unnecessary spectra.   
    7.8    Change of Window Display  
    						
    							7 - 15 
    7.9    Check of Photometric Value at Specified Wavelength   
     
    This is a function for shifting to the specified wavelength.    It is 
    usable for checking the optical axis, etc.   
    Open the monitor window and select the Set Wavelength (W) 
    command from the Spectrophotometer (S) menu or click the   
    (Set Wavelength) button.   
    A window as in Fig. 7-24 will open.   
     
     
     
    Fig. 7-24 
     
     
    Input target wavelength values and click OK.  
    Wavelength is now driven to the specified one and a photometric 
    value is read on the monitor window.    (Refer to (2) in 1.6.)   
     
     Wavelength drive to zero-order light 
    For checking the optical axis, etc. in the zero-order light or 
    moving the instrument, wavelength needs to be driven to the 
    zero-order light.    Open the window shown in Fig. 7-24 and 
    set wavelength at 0.    Then click OK, and wavelength will be 
    adjusted to the zero-order light.   
     
    NOTE:  For termination with wavelength kept at the zero-
    order light, select “Close the monitor window, but 
    keep the lamp operating?” in shutting down the 
    application (terminating the program).    “Close the 
    monitor window, but keep the lamp operating?” must 
    also be selected for turning off the photometer 
    power supply with the wavelength position kept 
    unchanged.  
    7.9  
    						
    							7 - 16 
    7.10    Collective Printing of Files   
     
    Wavelength scan data files (*.uds) and time scan data files 
    (*.udt) can be collectively printed.   
    From the File (F) menu, select the collective spectrum recording 
    (L) command.    A window as in Fig. 7-25 will appear.   
     
     
     
    Fig. 7-25 
     
     
    Click Select file.  
     
     
     
    Fig. 7-26 
     
     
    7.10    Collective Printing of Files  
    						
    							7 - 17 
    Specify the folder of a file to be printed at “Look In” and specify 
    the file.  Click Open (O).  
     
     
     
    Fig. 7-27 
     
     
    After check, click Print.  Printing starts.  The items to be 
    printed are the saved ones.    A maximum of 100 files can be 
    specified.  
    7.10  
    						
    							8 - 1 
    8.    MEASUREMENT USING OPTIONAL ACCESSORIES   
     
     
    For the cable connection method for each accessory, refer to the 
    instruction manual attached to the accessory.    Explanation is 
    given here on operations after setting of your analysis method, 
    which is required as instructed in Sections 2 to 5.   
     
    8.1    Use of Sample Sipper   
     
    Hook up the sample sipper to the spectrophotometer.     
    The parameters for the sipper are settable on its front panel.     
    Explained here is the procedure for creating a calibration curve 
    and measuring an unknown sample in the Photometry mode.   
     
    A message box appears in the standard measurement session, 
    so operate in accordance with the messages.    A message box 
    does not appear in the sample measurement session.   
    Measurement can be started just by pressing the sipping lever of 
    the sample sipper.   
     
    NOTES:  1.  When using the sample sipper, remeasurement, 
    interrupt measurement and blank measurement 
    cannot be made.    But remeasurement of 
    standards is possible.   
    2.  When repeat measurement is set, the standards 
    will be measured by the set number of times.   
    Samples will be measured only once.     
     
    Select the Measure command from the Spectrophotometer menu 
    or click the          (measurement) button on the toolbar, and the 
    window in Fig. 8-1 will open.     
     
     
     
    Fig. 8-1  8.1.1  When Not Using   
    a Sample Table   
     
    8.1.1  
    						
    							8 - 2 
    Press the sipping lever and measurement starts.    A message 
    box for the second measurement now appears.     
    For carrying out remeasurement or for skipping the second 
    standard measurement, select the relevant item with the mouse 
    (put a bullet in its radio button) and then click Yes.   
    When clicking No, the current measurement sequence will be 
    terminated.   
    For restarting measurement, click the    button.   
    Measurement then starts from the 1st standard.   
     
     
     
    Fig. 8-2 
     
     
    On completion of standard measurement, the window in Fig. 8-3 
    will open.   
     
     
     
    Fig. 8-3 
     
     
    8.1    Use of Sample Sipper  
    						
    							8 - 3 
    By clicking OK with the mouse, a calibration curve is drawn and 
    then samples can be measured.    When the window in Fig. 8-4 
    appears, you should press the sipping lever.     
    Measurement results appear at the area indicated by (1) in   
    Fig. 8-5.   
    By clicking Cancel, the measurement is terminated, and the 
    standards’ data is not saved.     
    Now select “Repeat the last measurement” and click OK.   
    Set the final standard in place and press the sipping lever.   
    When repeat measurement has been set, measurement is 
    started from the 1st one (Repl.No.1) for that standard.   
     
     
     
    Fig. 8-4 
     
     
     
     
    Fig. 8-5 
     
     
    When measurement is finished, click the End button, and the 
    data will be saved.   
    (1) 8.1.1  
    						
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