Hitachi F 2500 Manual
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7 - 11 7.7 Saving of Sample Table Sample tables can be saved. This is convenient for editing the sample table under the same name each time. Fig. 7-16 Sample Table After editing the sample table, click Save As and the window in Fig. 7-16 will appear. Enter a file name. For calling out the saved file (*.fls), click Load and select the file. Fig. 7-17 7.7
7 - 12 7.8 Change of Window Display When selecting the View (V) menu, display/non-display of toolbars and method of displaying multiple spectra can be selected. Monitor window Data processing window Fig. 7-20 View Menu Commands Scale Y Axis Up : Y axis scale is doubled for display. Scale Y Axis Down : Y axis scale is contracted by half for display. Reset Y Axis, Reset Axes : The scale set under the Monitor tab is taken. Autoscale Y Axis, Autoscale : Scale is adjusted to spectrum size for display. Display/ non-display setting 7.8 Change of Window Display
7 - 13 The method of displaying multiple spectra is selectable. Overlay Fig. 7-21 Stack Fig. 7-22 7.8
7 - 14 Tile Fig. 7-23 NOTE: When six, seven or more spectra are displayed, there is a possibility of the spectra becoming too small, or not all the traced values can be displayed. In this case, use the Overlay (O) command of Data (D) menu to delete unnecessary spectra. 7.8 Change of Window Display
7 - 15 7.9 Check of Photometric Value at Specified Wavelength This is a function for shifting to the specified wavelength. It is usable for checking the optical axis, etc. Open the monitor window and select the Set Wavelength (W) command from the Spectrophotometer (S) menu or click the (Set Wavelength) button. A window as in Fig. 7-24 will open. Fig. 7-24 Input target wavelength values and click OK. Wavelength is now driven to the specified one and a photometric value is read on the monitor window. (Refer to (2) in 1.6.) Wavelength drive to zero-order light For checking the optical axis, etc. in the zero-order light or moving the instrument, wavelength needs to be driven to the zero-order light. Open the window shown in Fig. 7-24 and set wavelength at 0. Then click OK, and wavelength will be adjusted to the zero-order light. NOTE: For termination with wavelength kept at the zero- order light, select “Close the monitor window, but keep the lamp operating?” in shutting down the application (terminating the program). “Close the monitor window, but keep the lamp operating?” must also be selected for turning off the photometer power supply with the wavelength position kept unchanged. 7.9
7 - 16 7.10 Collective Printing of Files Wavelength scan data files (*.uds) and time scan data files (*.udt) can be collectively printed. From the File (F) menu, select the collective spectrum recording (L) command. A window as in Fig. 7-25 will appear. Fig. 7-25 Click Select file. Fig. 7-26 7.10 Collective Printing of Files
7 - 17 Specify the folder of a file to be printed at “Look In” and specify the file. Click Open (O). Fig. 7-27 After check, click Print. Printing starts. The items to be printed are the saved ones. A maximum of 100 files can be specified. 7.10
8 - 1 8. MEASUREMENT USING OPTIONAL ACCESSORIES For the cable connection method for each accessory, refer to the instruction manual attached to the accessory. Explanation is given here on operations after setting of your analysis method, which is required as instructed in Sections 2 to 5. 8.1 Use of Sample Sipper Hook up the sample sipper to the spectrophotometer. The parameters for the sipper are settable on its front panel. Explained here is the procedure for creating a calibration curve and measuring an unknown sample in the Photometry mode. A message box appears in the standard measurement session, so operate in accordance with the messages. A message box does not appear in the sample measurement session. Measurement can be started just by pressing the sipping lever of the sample sipper. NOTES: 1. When using the sample sipper, remeasurement, interrupt measurement and blank measurement cannot be made. But remeasurement of standards is possible. 2. When repeat measurement is set, the standards will be measured by the set number of times. Samples will be measured only once. Select the Measure command from the Spectrophotometer menu or click the (measurement) button on the toolbar, and the window in Fig. 8-1 will open. Fig. 8-1 8.1.1 When Not Using a Sample Table 8.1.1
8 - 2 Press the sipping lever and measurement starts. A message box for the second measurement now appears. For carrying out remeasurement or for skipping the second standard measurement, select the relevant item with the mouse (put a bullet in its radio button) and then click Yes. When clicking No, the current measurement sequence will be terminated. For restarting measurement, click the button. Measurement then starts from the 1st standard. Fig. 8-2 On completion of standard measurement, the window in Fig. 8-3 will open. Fig. 8-3 8.1 Use of Sample Sipper
8 - 3 By clicking OK with the mouse, a calibration curve is drawn and then samples can be measured. When the window in Fig. 8-4 appears, you should press the sipping lever. Measurement results appear at the area indicated by (1) in Fig. 8-5. By clicking Cancel, the measurement is terminated, and the standards’ data is not saved. Now select “Repeat the last measurement” and click OK. Set the final standard in place and press the sipping lever. When repeat measurement has been set, measurement is started from the 1st one (Repl.No.1) for that standard. Fig. 8-4 Fig. 8-5 When measurement is finished, click the End button, and the data will be saved. (1) 8.1.1