Hitachi F7000 Instruction Manual
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5.2.2 5 - 7 14 Response When “Auto” is selected, response will be set automatically depending on scan speed. Select “Auto” usually. 15 Corrected spectra A function for determining the spectrum inherent to a sample by correcting the photometer wavelength characteristic using the saved instrument parameters, following measurement with the instrument parameters for photometer control. If there are no instrument parameters for the wavelength range to be measured, only the wavelength...
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5.2 Creating an Analysis Method 5 - 8 When selecting the Monitor tab, the window in Fig. 5-5 appears. For the settable range of each parameter, refer to Appendix G. Fig. 5-5 Monitor Tab Assign the following parameters. 1 Y-Axis Max (maximum) Enter a maximum value for Y-axis on the monitor window. 2 Y-Axis Min (minimum) Enter a minimum value for Y-axis on the monitor window. 3 Contour interval Function for setting intervals of drawing contour lines. 4 Open...
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5.2.3 5 - 9 NOTE: When the remaining memory capacity of PC in operation is very small (system resource is less than 20%), the data processing window will not open even if this item is turned ON. Either close the presently opened data processing window or restart the FL Solutions program. 5 Print report after data acquisition Select whether or not to print a report after sample measurement. When selected (check mark is applied), printing will be made automatically after measurement....
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5.2 Creating an Analysis Method 5 - 10 On selection of the Processing tab, the window in Fig. 5-6 will be displayed. For the settable range of each parameter, refer to Appendix G. Fig. 5-6 Processing Tab 1 Peak Finding: Integration method Select an integration method for the peaks to be displayed in the data processing window. 2 Threshold Set a detection limit for the photometric value axis of peak and valley. Peaks or valleys below the setting will not be detected....
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5.2.5 5 - 11 Select the Report tab, and the window in Fig. 5-7 will appear. Fig. 5-7 Report Tab 1 Output • Print Report A report will be printed. For printing method, refer to 5.9. • Use Microsoft(R) Excel Data will be transferred to Microsoft(R) Excel. For transferring method, refer to 7.13. • Use print generator sheet Select this method for using the report generator (option). For usage, refer to the instruction manual of the report generator. 2...
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5.2 Creating an Analysis Method 5 - 12 3 Print items (printable/transferable items) • Include date • Include instrument • Include graph When you put a check mark for this item, any of the graphs listed below is selectable. ◊ Contour ◊ Bird’s-eye view ◊ Contour and Bird’s-eye view ◊ Contour and Spectrum • Include peak table • Data listing ◊ Interval ◊ Start ◊ End These parameters are settable when “Use Microsoft(R) Excel” or “Use print generator sheet” is...
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5.3 5 - 13 5.3 Defining Your Samples A sample must be defined in the following procedure before measurement. (1) Click the (sample name/comment input) button on the Measurement toolbar. The window in Fig. 5-8 will appear. Fig. 5-8 (2) Make entries for Sample name and Comment. Maximum number of enterable characters (half-size) Sample name : 40 characters Comment : 255 characters For automatic saving, put a check mark in the “Auto File” box to specify a file...
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5.4 Conducting Measurement 5 - 14 5.4 Conducting Measurement (1) Make sure an analysis method has been set and a sample has been defined. (Refer to “5.2 Creating an Analysis Method” and “5.3 Defining Your Samples.”) (2) Set a sample in the sample compartment and click the button on the Measurement toolbar to start measurement. (See ① in Fig. 5-9.) On this monitor window, the X and Y axes stand for the EM and EX-side wavelengths, respectively. Fig. 5-9 Monitor...
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5.4 5 - 15 Fig. 5-10 (5) When measurement is completed, the data processing window appears as shown in Fig. 5-11. This is available only when a check mark is put for “Open data processing window after data acquisition” at the ‘Monitor’ tab of Analysis Method. (See ④ in Fig. 5-5.) The measured data will be saved automatically when auto saving is selected. If auto saving is not selected, select the “Save As” command from the File menu and save the data. Opening the saved...
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5.4 Conducting Measurement 5 - 16 Fig. 5-11 Data Processing Window (3-D scan) ① Contour lines From these contour lines, excitation and emission spectra can be read out. As the cursor is moved, the cursor-specified excitation and emission spectra are displayed in ② and ③. ② Excitation spectrum An excitation spectrum at the cursor position in ① is displayed. Wavelength and photometric value can be read by selecting the “trace” command from the View menu or clicking the...
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