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Hitachi F7000 Instruction Manual

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Page 181

5.2.2 
5 - 7 
14 Response  
When “Auto” is selected, response will be set automatically 
depending on scan speed.    Select “Auto” usually.   
15 Corrected spectra   
A function for determining the spectrum inherent to a sample by 
correcting the photometer wavelength characteristic using the 
saved instrument parameters, following measurement with the 
instrument parameters for photometer control.    If there are no 
instrument parameters for the wavelength range to be measured, 
only the wavelength...

Page 182

5.2    Creating an Analysis Method 
5 - 8 
When selecting the Monitor tab, the window in Fig. 5-5 appears.     
For the settable range of each parameter, refer to Appendix G.   
 
 
 
Fig. 5-5  Monitor Tab 
 
 
Assign the following parameters.   
 
1 Y-Axis Max (maximum)   
Enter a maximum value for Y-axis on the monitor window.   
2 Y-Axis Min (minimum)   
Enter a minimum value for Y-axis on the monitor window.   
3 Contour interval   
Function for setting intervals of drawing contour lines.     
4 Open...

Page 183

5.2.3 
5 - 9 
NOTE:  When the remaining memory capacity of PC in operation is 
very small (system resource is less than 20%), the data 
processing window will not open even if this item is turned ON.   
Either close the presently opened data processing window or 
restart the FL Solutions program.   
 
5 Print report after data acquisition   
Select whether or not to print a report after sample measurement.   
When selected (check mark is applied), printing will be made 
automatically after measurement....

Page 184

5.2    Creating an Analysis Method 
5 - 10 
On selection of the Processing tab, the window in Fig. 5-6 will be 
displayed.  
For the settable range of each parameter, refer to Appendix G.   
 
 
 
Fig. 5-6  Processing Tab 
 
 
1 Peak Finding:  Integration method  
Select an integration method for the peaks to be displayed in the 
data processing window.   
2 Threshold  
Set a detection limit for the photometric value axis of peak and 
valley.    Peaks or valleys below the setting will not be detected....

Page 185

5.2.5 
5 - 11 
Select the Report tab, and the window in Fig. 5-7 will appear.   
 
 
 
Fig. 5-7  Report Tab 
 
 
1 Output  
• Print Report   
A report will be printed.    For printing method, refer to 5.9.   
• Use Microsoft(R) Excel   
Data will be transferred to Microsoft(R) Excel.    For transferring 
method, refer to 7.13.   
• Use print generator sheet   
Select this method for using the report generator (option).     
For usage, refer to the instruction manual of the report 
generator.  
2...

Page 186

5.2    Creating an Analysis Method 
5 - 12 
3 Print items (printable/transferable items) 
• Include date   
• Include instrument 
• Include graph   
When you put a check mark for this item, any of the graphs 
listed below is selectable.   
◊ Contour  
◊ Bird’s-eye view  
◊  Contour and Bird’s-eye view   
◊  Contour and Spectrum   
• Include peak table   
• Data listing   
◊ Interval  
◊ Start  
◊ End  
These parameters are settable when “Use Microsoft(R) Excel” 
or “Use print generator sheet” is...

Page 187

5.3 
5 - 13 
5.3  Defining Your Samples  
 
A sample must be defined in the following procedure before 
measurement.  
 
(1) Click the 
  (sample name/comment input) button on the 
Measurement toolbar.    The window in Fig. 5-8 will appear.   
 
 
 
Fig. 5-8 
 
 
(2)  Make entries for Sample name and Comment.   
Maximum number of enterable characters (half-size)   
Sample name :  40 characters   
Comment : 255 characters  
 
For automatic saving, put a check mark in the “Auto File” box to 
specify a file...

Page 188

5.4  Conducting Measurement 
5 - 14 
5.4  Conducting Measurement  
 
(1)  Make sure an analysis method has been set and a sample has 
been defined.    (Refer to “5.2 Creating an Analysis Method” and 
“5.3 Defining Your Samples.”)   
 
(2)  Set a sample in the sample compartment and click the 
 
button on the Measurement toolbar to start measurement.     
(See ①  in Fig. 5-9.)   
On this monitor window, the X and Y axes stand for the EM and 
EX-side wavelengths, respectively.   
 
 
 
Fig. 5-9  Monitor...

Page 189

5.4 
5 - 15 
 
 
 
Fig. 5-10 
 
 
(5)  When measurement is completed, the data processing window 
appears as shown in Fig. 5-11.    This is available only when a 
check mark is put for “Open data processing window after data 
acquisition” at the ‘Monitor’ tab of Analysis Method.    (See ④ in 
Fig. 5-5.)   
The measured data will be saved automatically when auto saving 
is selected.   
If auto saving is not selected, select the “Save As” command from 
the File menu and save the data.    Opening the saved...

Page 190

5.4  Conducting Measurement 
5 - 16 
 
 
 
 
 
Fig. 5-11    Data Processing Window (3-D scan) 
 
 
① Contour lines  
From these contour lines, excitation and emission spectra can be 
read out.   
As the cursor is moved, the cursor-specified excitation and 
emission spectra are displayed in ② and ③.  
 
② Excitation spectrum  
An excitation spectrum at the cursor position in ① is displayed.  
Wavelength and photometric value can be read by selecting the 
“trace” command from the View menu or clicking the...
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