Hitachi F7000 Instruction Manual

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(cont’d) 
Parameter Name  Setting Range 
Response (unit: s)  0.002 
0.004 
0.01 
0.05 
0.1 
0.5 
2.0 
4.0 
8.0 
Auto 
Corrected spectra  ON, OFF 
Shutter control  ON, OFF 
Replicates  2 to 99 
Cycle time  2 to 3600 s 
 
ON :  Checked 
OFF :  Unchecked 
 
 
G.5.2  3-D Time Scan:    Monitor Tab 
 
Parameter Name  Setting Range 
Y Axis: Max  -119999999.9 to 120000000.0 
Y Axis: Min  -120000000.0 to 119999999.9 
Contour interval  0.001 to 1000 
Open data processing window after data acquisition  ON,...

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G.5.4  3D Time Scan:    Report Tab 
 
Parameter Name  Setting Range 
Output  Print Report, Use Microsoft(R) Excel, Use print 
generator sheet 
Orientation Portrait, Landscape 
Print items: Include date  ON, OFF 
Print items: Include instrument  ON, OFF 
Print items: Include graph  ON, OFF 
ON: Any of the following items are selectable. 
• Contour 
• Bird’s-eye view 
•  Contour and Bird’s-eye view 
•  Contour and Spectrum 
Print items: Data listing*1 ON, OFF 
ON:  Setting can be made for time scan...

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APPENDIX H  SAMPLING INTERVAL 
 
H.1  Wavelength Scan 
 
The data sampling interval is set as follows according to the scan speed. 
 
[Data mode = Fluorescence/Luminescence] 
 
Scan Speed (nm/min) Sampling Interval (nm) 
60000 2.0 
30000 1.0 
12000 0.2 
2400 0.2 
1200 0.2 
240 0.2 
60 0.2 
30 0.2 
 
 
[Data mode = Phosphorescence, Chopping speed = 40 Hz] 
 
Scan Speed (nm/min) Sampling Interval (nm) 
240 0.2 
60 0.2 
30 0.2 
 
 
[Data mode = Phosphorescence, Chopping speed = 20/10 Hz] 
 
Scan...

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H.2  Time Scan 
 
The data sampling interval is set as follows according to the scan time. 
 
[Data mode = Fluorescence/Luminescence/Phosphorescence/ 
Phosphorescence Life Time] 
 
Sampling Interval [ms] 
Phosphorescence 
Mode/Chopping Speed Scan Time   
[s] Fluorescence/Luminescence/
Phosphorescence  
Life Time Mode 
40 Hz  20 Hz  10 Hz 
0.1 ~ 1  1  50  100  200 
~ 3  1  50  100  200 
~ 7  2  50  100  200 
~ 18  5  50  100  200 
~ 36  10  50  100  200 
~ 72  20  50  100  200 
~ 180  50  50  100...

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H.3  3-D Time Scan 
 
The data sampling interval is set as follows according to the scan speed. 
 
[Data mode = Fluorescence/Luminescence] 
 
Scan Speed (nm/min) Sampling Interval (nm) 
60000 2.0 
30000 1.0 
12000 1.0 
2400 1.0 
1200 1.0 
240 1.0 
60 1.0 
30 1.0 
 
 
[Data mode = Phosphorescence, Chopping speed = 40 Hz] 
 
Scan Speed (nm/min) Sampling Interval (nm) 
240 1.0 
60 1.0 
30 1.0 
 
 
[Data mode = Phosphorescence, Chopping speed = 20/10 Hz] 
 
Scan Speed (nm/min) Sampling Interval (nm)...

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APPENDIX I  PARAMETER SETTING RANGE 
ON OPTIONS WINDOW 
 
I.1  Display Tab 
 
Parameter Name  Setting Range 
Show trace display  ON, OFF 
Show gridlines with 
increment ON, OFF 
ON:  Gridline width is selectable from 
Wide, Middle and Narrow. 
Display items:   
Wavelength scan Show graph only,   
Show graph plus peak table 
Display items:   
Time scan Show graph only,   
Show graph plus kinetic data,   
Show graph plus peak table 
Display items:   
3-D Scan Show contour plus EX, EM spectrum,...

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I.2  Processing Tab 
 
Parameter Name  Setting Range 
Integration method  Rectangular, Trapezoid, Romberg 
Calibration formula  Data = f(Conc), Conc = f(Data) 
Data output to peak table  ON, OFF 
Smoothing: Processing  Savitsky-Golay, Mean, Median 
Smoothing: Order  2 to 4 
Smoothing: Number of points  5 to 101 
Derivative: Smoothing order  2 to 4 
Derivative: Smoothing order  5 to 101 
 
 
I.3  Analysis Condition Tab 
 
Parameter Name  Setting Range 
Integration time for current data  0.1 to...

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APPENDIX J    ERROR MESSAGE LIST 
 
Error Message  Probable Cause  Remedy 
ROM Error    ROM error has occurred.  Contact our local service office. 
RAM Error    RAM error has occurred.  Contact our local service office. 
Lamp is not lighted  Lamp extinguished during 
initialization. Replace the lamp. 
Power interruption  Momentary power failure 
detected at instrument. Check the connection of USB cable, 
and start up PC and 
spectrophotometer again.  If error 
recurs, contact our local service...

INDEX - 1 
INDEX 
1st order (linear calibration curve) ............................................................................................... 4-12, A-1 
3-D scan ........................................................................................................................................ 1-2, 5-1 
3-D time scan ....................................................................................................................... 1-2, 1-27, 6-1 
3rd order (Cubic working curve)...

INDEX - 2 
Contour ...................................................................................................................... 1-2, 1-25, 5-19, 6-18 
Contour interval .................................................................................................................................... 5-8 
Corrected spectrum ............................................................................................. 1-28, 2-7, 5-7, 6-7, A-26 
Cycle time...